Applications
Quantification of Carbamates Fungicides in Beverage by LC/MS/MS
20025
Molluscacides
Food & Beverage
Product / Trade Good
Product / Trade Good
Environmental / Health
Therapeutic / Clinical
Environmental / Health

Applications

Quantification of Carbamates Fungicides in Beverage by LC/MS/MS
Analytes
1
2
3
4
5
6
7
8
Compound Name
Aldoxycarb
CID
9570093
Molecular Formula
C7H14N2O4S
Molecular Weight
222
No. Hydrogen Bond Acceptors
5
No. Hydrogen Bond Donors
1
Details
LC Conditions (App ID: 20025)
Elution Type:
Gradient
Mobile Phase:
A: 5mM ammonium formate
B: 5mM ammonium formate in acetonitrile
Gradient Profile:
Step No.Time(min)%A%B
108515
22.5595
34595
44.018515
588515
Flow Rate:
0.5 mL/min
Temperature:
28°C
Detection:
Tandem Mass Spec (MS-MS) @ 22°C
Sample Preparation Details
SPE Condition 1:
1 mL Methanol
SPE Condition 2:
1 mL 25 mM Ammonium acetete pH 5.5
SPE Load:
Load 1.40 mL Sample diluted in pretreated sample
SPE Wash 1:
1 mL 25 mM Ammonium acetete pH 5.5
SPE Wash 2:
1 mL Methanol/Water (15:85)
SPE Dry:
2 min at 10mm Hg
SPE Elution 1:
0.5 mL 5% Formic acid in Methanol
SPE Evaporation:
Evaporate to dryness
SPE Reconstitute:
1 mL Initial mobile phase