Applications
Extraction of Carbamate Pesticides using Strata-X on Kinetex 2.6µm C18 50 x 2.1mm ID by LCMS
18638
Separation Mode: Reversed Phase
Reversed Phase
C18
HPLC
Molluscacides

Applications

Extraction of Carbamate Pesticides using Strata-X on Kinetex 2.6µm C18 50 x 2.1mm ID by LCMS

Analytes

1
2
3
4
5
6
7
8
Compound Name
Temik Sulfoxide
CID
9568700
Molecular Formula
C7H14N2O3S
Molecular Weight
206
No. Chiral Centers:
1
No. Hydrogen Bond Acceptors
4
No. Hydrogen Bond Donors
1

Conditions

LC Conditions (App ID: 18638)
Column:Kinetex 2.6 µm C18 100 Å, LC Column 50 x 2.1 mm, Ea
Brand Name:Kinetex
Part No:00B-4462-AN
Elution Type:Gradient
Mobile Phase:A: 5mM Ammonium formate in H2O
B: mM Ammonium formate in ACN
Gradient Profile:
Step No.Time(min)%A%B
10973
20.25973
32.5595
44595
54.01973
65.5973
Flow Rate:500 µL/min
Temperature:25°C
Detection:Mass Spectrometer (MS) amu @ 22°C

Sample Preparation Details
Description:Strata-X 33 µm Polymeric Reversed Phase, 30 mg / 3 mL, Tubes, 50/Pk
Part Number:8B-S100-TBJ
SPE Condition 1:1 mL Methanol at 2 mL/min
SPE Condition 2:1 mL 25 mM ammonium acetate pH 5.5 at 2 mL/min
SPE Load:Load 0.40 mL Sample diluted in 1
SPE Wash 1:1 mL 25 mM ammonium acetate pH 5.5 at 2 mL/min
SPE Wash 2:1 mL 15% methanol at 2 mL/min
SPE Dry:2 mins at 10" of Hg
SPE Elution 1:0.5 mL 5% formic acid/methanol at 1 mL/min
SPE Elution 2:0.5 mL 5% formic acid/methanol at 1 mL/min
SPE Evaporation:Evaporate to dryness
SPE Reconstitute:200 µL 97/3 initial LC mobile phase

Order Items Used in This Application

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